{"id":1123,"date":"2019-07-19T15:07:00","date_gmt":"2019-07-19T13:07:00","guid":{"rendered":"http:\/\/www.microgels.rwth-aachen.de\/?p=1123"},"modified":"2020-01-08T14:53:32","modified_gmt":"2020-01-08T13:53:32","slug":"closing-the-1-5-%ce%bcm-size-gap-temperature-programmed-fed-batch-synthesis-of-%ce%bcm-sized-microgels","status":"publish","type":"post","link":"https:\/\/www.microgels.rwth-aachen.de\/?p=1123","title":{"rendered":"Closing the 1\u20135 \u03bcm size gap: Temperature-programmed, fed-batch synthesis of \u03bcm-sized microgels"},"content":{"rendered":"\n<div class=\"wp-block-image\"><figure class=\"aligncenter size-large is-resized\"><a href=\"http:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung.png\"><img loading=\"lazy\" decoding=\"async\" src=\"http:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung-1024x563.png\" alt=\"\" class=\"wp-image-1125\" width=\"540\" height=\"297\" srcset=\"https:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung-1024x563.png 1024w, https:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung-300x165.png 300w, https:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung-768x422.png 768w, https:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung.png 1391w\" sizes=\"auto, (max-width: 540px) 100vw, 540px\" \/><\/a><\/figure><\/div>\n\n\n\n<p>In this paper, we present the fed-batch synthesis of microgels in the 1-5 \u00b5m size range. We backed up experimental results with simulations based on mechanistic models. We synthesize specific microgel structures with a minimal number of trial experiment by predicting the required synthesis procedure using model-based simulation and optimization. In the fed-batch experiments presented here, we achieve good agreement with experimental data and are able to determine reasons for the observed increase in the microgel size.<\/p>\n\n\n\n<p><em>Agnieszka N. Ksiazkiewicz, Luise Bering, Falco Jung, Nadja A. Wolter, J\u00f6rn Viell, Alexander Mitsos and Andrij Pich<\/em><\/p>\n\n\n\n<p>Please refer to DOI <a href=\"http:\/\/dx.doi.org\/10.1016\/j.cej.2019.122293\">10.1016\/j.cej.2019.122293<\/a> for more information.<\/p>\n","protected":false},"excerpt":{"rendered":"<p>In this paper, we present the fed-batch synthesis of microgels in the 1-5 \u00b5m size range. We backed up experimental<\/p>\n","protected":false},"author":3,"featured_media":1125,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"advgb_blocks_editor_width":"","advgb_blocks_columns_visual_guide":"","footnotes":""},"categories":[34],"tags":[],"class_list":["post-1123","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-highlights"],"author_meta":{"display_name":"Anna Eisele","author_link":"https:\/\/www.microgels.rwth-aachen.de\/?author=3"},"featured_img":"https:\/\/www.microgels.rwth-aachen.de\/wp-content\/uploads\/2019\/12\/graphicalAbstract_Ksiak_Jung-300x165.png","coauthors":[],"tax_additional":{"categories":{"linked":["<a href=\"https:\/\/www.microgels.rwth-aachen.de\/?cat=34\" class=\"advgb-post-tax-term\">Highlights<\/a>"],"unlinked":["<span class=\"advgb-post-tax-term\">Highlights<\/span>"]}},"comment_count":"0","relative_dates":{"created":"Posted 7 years ago","modified":"Updated 6 years ago"},"absolute_dates":{"created":"Posted on July 19, 2019","modified":"Updated on January 8, 2020"},"absolute_dates_time":{"created":"Posted on July 19, 2019 15:07","modified":"Updated on January 8, 2020 14:53"},"featured_img_caption":"","series_order":"","_links":{"self":[{"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/posts\/1123","targetHints":{"allow":["GET"]}}],"collection":[{"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/users\/3"}],"replies":[{"embeddable":true,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=1123"}],"version-history":[{"count":4,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/posts\/1123\/revisions"}],"predecessor-version":[{"id":1359,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/posts\/1123\/revisions\/1359"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=\/wp\/v2\/media\/1125"}],"wp:attachment":[{"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=1123"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=1123"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.microgels.rwth-aachen.de\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=1123"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}